Copper in PDB 4m4j: Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy

The structure of Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy, PDB code: 4m4j was solved by C.G.Frankaer, P.Harris, K.Stahl, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	16.75 / 1.90
Space group	H 3
Cell size a, b, c (Å), α, β, γ (°)	80.650, 80.650, 33.313, 90.00, 90.00, 120.00
R / Rfree (%)	16.9 / 22

The binding sites of Copper atom in the Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy (pdb code 4m4j). This binding sites where shown within 5.0 Angstroms radius around Copper atom.
In total 2 binding sites of Copper where determined in the Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy, PDB code: 4m4j:
Jump to Copper binding site number: 1; 2;

Copper binding site 1 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 1 of Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ B:Cu101 b:14.1 occ:0.33 NE2 B:HIS10 2.0 9.8 1.0 O B:HOH206 2.2 22.2 1.0 CE1 B:HIS10 2.9 11.2 1.0 CD2 B:HIS10 3.1 8.4 1.0 O B:HOH211 3.8 25.5 1.0 ND1 B:HIS10 4.0 15.4 1.0 CG B:HIS10 4.2 13.7 1.0 O B:HOH213 4.6 32.2 1.0 O D:HOH224 4.6 41.4 0.3

Copper binding site 2 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 2 of Radiation Damage Study of Cu T6-Insulin - 0.30 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ D:Cu101 b:18.3 occ:0.33 NE2 D:HIS10 2.0 16.5 1.0 CE1 D:HIS10 3.0 14.8 1.0 CD2 D:HIS10 3.0 12.5 1.0 O D:HOH212 3.5 30.8 0.3 ND1 D:HIS10 4.1 16.3 1.0 CG D:HIS10 4.1 16.2 1.0 O D:HOH220 4.1 36.6 1.0

C.G.Frankaer, S.Mossin, K.Stahl, P.Harris. Towards Accurate Structural Characterization of Metal Centres in Protein Crystals: the Structures of Ni and Cu T6 Bovine Insulin Derivatives. Acta Crystallogr.,Sect.D V. 70 110 2014.
ISSN: ISSN 0907-4449
PubMed: 24419384
DOI: 10.1107/S1399004713029040