Copper in PDB 4m4h: Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy

The structure of Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy, PDB code: 4m4h was solved by C.G.Frankaer, P.Harris, K.Stahl, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	16.75 / 1.90
Space group	H 3
Cell size a, b, c (Å), α, β, γ (°)	80.658, 80.658, 33.333, 90.00, 90.00, 120.00
R / Rfree (%)	16.6 / 22

The binding sites of Copper atom in the Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy (pdb code 4m4h). This binding sites where shown within 5.0 Angstroms radius around Copper atom.
In total 2 binding sites of Copper where determined in the Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy, PDB code: 4m4h:
Jump to Copper binding site number: 1; 2;

Copper binding site 1 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 1 of Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ B:Cu101 b:15.9 occ:0.33 NE2 B:HIS10 2.0 12.4 1.0 O B:HOH209 2.0 29.3 1.0 CE1 B:HIS10 2.9 19.4 1.0 CD2 B:HIS10 3.1 10.2 1.0 O B:HOH206 3.8 26.9 1.0 ND1 B:HIS10 4.1 19.9 1.0 CG B:HIS10 4.2 17.0 1.0 O B:HOH212 4.5 31.6 1.0 O B:HOH220 4.9 41.7 0.3

Copper binding site 2 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 2 of Radiation Damage Study of Cu T6-Insulin - 0.06 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ D:Cu101 b:20.3 occ:0.33 NE2 D:HIS10 2.0 17.1 1.0 O D:HOH216 2.5 36.4 1.0 CD2 D:HIS10 3.0 15.2 1.0 CE1 D:HIS10 3.0 16.8 1.0 O D:HOH214 4.1 34.1 1.0 ND1 D:HIS10 4.1 16.5 1.0 CG D:HIS10 4.1 18.7 1.0

C.G.Frankaer, S.Mossin, K.Stahl, P.Harris. Towards Accurate Structural Characterization of Metal Centres in Protein Crystals: the Structures of Ni and Cu T6 Bovine Insulin Derivatives. Acta Crystallogr.,Sect.D V. 70 110 2014.
ISSN: ISSN 0907-4449
PubMed: 24419384
DOI: 10.1107/S1399004713029040