Copper in PDB 4m4f: Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy

The structure of Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy, PDB code: 4m4f was solved by C.G.Frankaer, P.Harris, K.Stahl, with X-Ray Crystallography technique. A brief refinement statistics is given in the table below:

Resolution Low / High (Å)	16.28 / 1.90
Space group	H 3
Cell size a, b, c (Å), α, β, γ (°)	81.130, 81.130, 33.469, 90.00, 90.00, 120.00
R / Rfree (%)	16.6 / 23.5

The binding sites of Copper atom in the Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy (pdb code 4m4f). This binding sites where shown within 5.0 Angstroms radius around Copper atom.
In total 2 binding sites of Copper where determined in the Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy, PDB code: 4m4f:
Jump to Copper binding site number: 1; 2;

Copper binding site 1 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 1 of Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ B:Cu101 b:18.2 occ:0.33 O B:HOH203 1.9 26.0 1.0 NE2 B:HIS10 2.0 16.6 1.0 CE1 B:HIS10 3.0 23.5 1.0 CD2 B:HIS10 3.0 12.7 1.0 O B:HOH206 3.7 28.5 1.0 ND1 B:HIS10 4.1 21.8 1.0 CG B:HIS10 4.1 13.5 1.0 O B:HOH217 4.7 36.3 1.0 O D:HOH230 4.8 48.9 0.3

Copper binding site 2 out of 2 in the Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy


Mono view


Stereo pair view

A full contact list of Copper with other atoms in the Cu binding site number 2 of Radiation Damage Study of Cu T6-Insulin - 0.01 Mgy within 5.0Å range: probe atom residue distance (Å) B Occ D:Cu101 b:20.3 occ:0.33 NE2 D:HIS10 2.0 19.7 1.0 CE1 D:HIS10 2.9 20.9 1.0 O D:HOH229 3.0 47.5 1.0 CD2 D:HIS10 3.1 14.9 1.0 ND1 D:HIS10 4.1 17.3 1.0 CG D:HIS10 4.2 17.9 1.0 O D:HOH219 4.2 38.7 1.0 O D:HOH225 4.5 43.1 1.0 O D:HOH207 4.9 33.1 1.0

C.G.Frankaer, S.Mossin, K.Stahl, P.Harris. Towards Accurate Structural Characterization of Metal Centres in Protein Crystals: the Structures of Ni and Cu T6 Bovine Insulin Derivatives. Acta Crystallogr.,Sect.D V. 70 110 2014.
ISSN: ISSN 0907-4449
PubMed: 24419384
DOI: 10.1107/S1399004713029040